EBOOK KIMIA ANALITIK DASAR

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Ebook Kimia Analitik Dasar

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This results in a white precipitate in which NH 4OH is added. The tests are conducted in presence of dilute HCl to keep the S2- ion concen-tration at a minimum level. This round of tests helps only in second 2nd gro-up cations precipitation.

The cations precipitation of the 4th group if present in the solution might occur in the absence of dilute HCl which can give wrong results. The use of sulphuric acid and nitric acid can cause to the precipitation of the 4th group cations and formation of colloidal sulphur respectively.

This group is determined by the addition of the respective salt in water and then adding dilute HCl and then follow it by adding H2S. However they form precipitates with ammonium sulphides NH4 2S in neutral or ammonical medium. They precipitate with ammonium carbonate NH4 CO3 in the pre-sence of ammonium chloride in neutral medium. The result of experiment and the presence of the respective ions are shown in the table below.

It can be identified by special reaction or by flame test. Sodium and potassium ion are from group IA Alkaline , and they have similarity. Both of them are big enough, colourless, can not reduced in solution state, so it can not react with water. Anions The methods available for the detection of anions are not as systematic as those which have been described above for cations.

No really satisfactory scheme has yet been proposed which permits the separation of the common anions into major groups, and the subsequent unequivocal separation of each group into its independent constituents; however, it is possible to detect anions individually in most cases, after perhaps a stage separation. It is advantageous to remove all heavy metals from the sample by extracting the anions through boiling with sodium carbonate solution; heavy metal ions are Experiment Report: Analysis of Anions and Cations 19 precipitated out in the form of carbonates, while the anions remain in solution accompanied by sodium ions.

The following scheme of classification of anions has been found to work well in practice; anions are divided into four groups on the basis of their reactions with di-lute hydrochloric acid and of the differences of solubilities of their barium and sil-ver salts. However, they form precipitates with silver ions in dilute nitric acid medium.

To identify nitrate ion can be done by brown ring test which can be done by adding concentrate H2S04 and then adding saturated FeSO4 little by little through the tube wall.

Tools and Material A.

Tools B. Materials 1. Test tube 1. Sample NH4NO3 2. Pipettes 2. NaOH solution 3. Litmus paper 3. Saturated Na2CO3 4.

Test tube rack 4. Concentrated H2SO4 5.

Filter paper 5. Saturated FeSO4 6. Tripod 7. Funnel 8.

Beaker glass 9. Bunsen burner VII. Flow Chart A. Analysis Experiment Report: Analysis of Anions and Cations In this experiment we got sample number two which has form colourless crystal through random selection. First of all we are dividing the sample into three with ratio First, we are entering some of the sample into reaction tube.Vg tergantung pada temperatur, koef.

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